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Description Degradation/erosion of the free‐standing samples with a thickness of a) 190 µm, b) 370 µm, and c) 670 µm monitored gravimetrically. The data acquired was fitted by a single exponential function...
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics -
Description SPR setup: polarized light is coupled through a prism (via an index‐matching oil layer, an LaSFN9 glass slide, and chromium adhesion layer) into a gold layer (orange). The gold substrate is covered...
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics -
Description Degradation/erosion of a PSA film with d0 = 166 nm monitored by ellipsometry, SPR, and FTIR. The data points at time t were normalized to t0. a) the angular reflectivity curve at t = 14 h obtained...
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics -
Description Overview of the poly(sebacic anhydride) (PSA) samples with different thicknesses obtained by spin‐coating, doctor‐blading, or compression‐molding; the amounts of sample used in each case; and the...
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics -
Description Rate constants obtained from the exponential and linearized fits to the ellipsometry, SPR, FTIR, and gravimetry data
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics -
Description AFM height images of PSA thin films on silicon wafers after different degradation times (sample thickness at 0 h: 166 nm). Scale bars: 1 µm. Roughness values Rq are given underneath the images....
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics -
Description Degradation/erosion of the 378 nm thick PSA film monitored by a) ellipsometry and b) FTIR, and c) degradation/erosion of the 450 nm thick film monitored by FTIR. The data points at time t were...
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics -
Description a) Plot of log (initial layer thickness in nm) versus apparent degradation rate constants kapp (obtaind by fitting the data with a single exponential function). Literature data from ref. was also...
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics -
Description Synthesis of poly(sebacic anhydride). The sebacic acid was activated with acetic anhydride and then melt‐polymerized to give poly(sebacic anhydride).
Article Title: Degradation of Polymer Films on Surfaces: A Model Study with Poly(sebacic anhydride)
Publication Title: Macromolecular Chemistry and Physics